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1 article(s) from Lasso, Juan D

Synthesis of α-(perfluoroalkylsulfonyl)propiophenones: a new set of reagents for the light-mediated perfluoroalkylation of aromatics

Durbis J. Castillo-Pazos,
Juan D. Lasso and
Chao-Jun Li

Beilstein J. Org. Chem. 2022, 18, 788–795, doi:10.3762/bjoc.18.79

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Scheme 1: Envisioned Minisci perfluoroalkylation facilitated by “dummy group” reagents 1a–c.

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Scheme 2: Control experiments for the nucleophilic substitution of perfluoroalkylsulfinates 2 and halogenated...

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Scheme 3: Left: isolated yields of synthesized perfluoroalkylating reagents: perfluorobutyl (1a), perfluorohe...

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Scheme 4: Radical trapping experiment with 1,1-diphenylethylene (7) and 1b confirming the initially proposed ...

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Scheme 5: Demonstrative scope for the perfluoroalkylation of aromatics. Isolated yields are shown in parenthe...

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Published 04 Jul 2022

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